Simple method for the handling of crystals at low temperature: Application to the X-ray structure determination of Bu t 2 P(=NSiMe 3 )NHSiMe 3 and Bu t 2 P(NSiMe 3 ) 2
| dc.contributor.author | Edwards, Alison | |
| dc.contributor.author | Wenger, Eric | |
| dc.date.accessioned | 2015-12-13T22:22:53Z | |
| dc.date.available | 2015-12-13T22:22:53Z | |
| dc.date.issued | 2002 | |
| dc.date.updated | 2015-12-11T08:00:54Z | |
| dc.description.abstract | Crystals of the very soluble iminophosphonamide species Bu2tP(=NSiMe3)NHSiMe3 (1) and [But2P(NSiMe3)2]Li·(thf)2 (2) have been obtained and were mounted at dry-ice temperature using a propan-2-ol matrix for X-ray data collection at 100 K. This very simple | |
| dc.identifier.issn | 0004-9425 | |
| dc.identifier.uri | http://hdl.handle.net/1885/72492 | |
| dc.publisher | CSIRO Publishing | |
| dc.source | Australian Journal of Chemistry | |
| dc.subject | Keywords: Catalysis; Chelation; Crystal growth; Low temperature engineering; Molecular structure; X ray diffraction; X ray diffraction analysis; Chemical decomposition; Crystal handling; Ligand; X ray structures; Crystal structure | |
| dc.title | Simple method for the handling of crystals at low temperature: Application to the X-ray structure determination of Bu t 2 P(=NSiMe 3 )NHSiMe 3 and Bu t 2 P(NSiMe 3 ) 2 | |
| dc.type | Journal article | |
| local.bibliographicCitation.lastpage | 252 | |
| local.bibliographicCitation.startpage | 249 | |
| local.contributor.affiliation | Edwards, Alison, College of Physical and Mathematical Sciences, ANU | |
| local.contributor.affiliation | Wenger, Eric, College of Physical and Mathematical Sciences, ANU | |
| local.contributor.authoremail | repository.admin@anu.edu.au | |
| local.contributor.authoruid | Edwards, Alison, u9900186 | |
| local.contributor.authoruid | Wenger, Eric, u9205509 | |
| local.description.notes | Imported from ARIES | |
| local.description.refereed | Yes | |
| local.identifier.absfor | 030606 - Structural Chemistry and Spectroscopy | |
| local.identifier.ariespublication | MigratedxPub3275 | |
| local.identifier.citationvolume | 55 | |
| local.identifier.doi | 10.1071/CH02016 | |
| local.identifier.scopusID | 2-s2.0-10844295026 | |
| local.identifier.uidSubmittedBy | Migrated | |
| local.type.status | Published Version |