Simple method for the handling of crystals at low temperature: Application to the X-ray structure determination of Bu  t   2 P(=NSiMe 3 )NHSiMe 3  and Bu  t   2 P(NSiMe 3 ) 2

Edwards, Alison; Wenger, Eric

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Simple method for the handling of crystals at low temperature: Application to the X-ray structure determination of Bu t 2 P(=NSiMe 3 )NHSiMe 3 and Bu t 2 P(NSiMe 3 ) 2

Date

2002

Authors

Edwards, Alison

Wenger, Eric

Publisher

CSIRO Publishing

Abstract

Crystals of the very soluble iminophosphonamide species Bu2tP(=NSiMe3)NHSiMe3 (1) and [But2P(NSiMe3)2]Li·(thf)2 (2) have been obtained and were mounted at dry-ice temperature using a propan-2-ol matrix for X-ray data collection at 100 K. This very simple