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Direct detection of boldenone sulfate and glucuronide conjugates in horse urine by ion trap liquid chromatography-mass spectrometry

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dc.contributor.authorPu, Fan
dc.contributor.authorMcKinney, Andrew
dc.contributor.authorStenhouse, Allen M
dc.contributor.authorSuann, Craig J
dc.contributor.authorMcLeod, Malcolm
dc.date.accessioned2015-12-10T22:24:17Z
dc.date.issued2004
dc.date.updated2015-12-09T09:15:46Z
dc.description.abstractA study of the equine phase II metabolism of the anabolic agent boldenone is reported. Boldenone sulfate, boldenone glucuronide and their C17-epimers were synthesised as reference standards in our lab and a method was developed for their detection in a horse urine matrix. Solid phase extraction was used to purify the analytes, which were then detected by ion trap LC/MS. Negative and positive ionisation mode MS2 were used for the detection of sulfate and glucuronide conjugates, respectively. Boldenone sulfate and 17-epiboldenone glucuronide were detected as the major and minor phase II metabolites, respectively, in horse urine samples collected following the administration of boldenone undecylenate by intramuscular injection.
dc.identifier.issn1570-0232
dc.identifier.urihttp://hdl.handle.net/1885/53184
dc.publisherElsevier
dc.sourceJournal of Chromatography B
dc.titleDirect detection of boldenone sulfate and glucuronide conjugates in horse urine by ion trap liquid chromatography-mass spectrometry
dc.typeJournal article
local.bibliographicCitation.issue1-2
local.bibliographicCitation.lastpage246
local.bibliographicCitation.startpage241
local.contributor.affiliationPu, Fan, University of Sydney
local.contributor.affiliationMcKinney, Andrew, Australian Racing Forensic Laboratory
local.contributor.affiliationStenhouse, Allen M, Australian Racing Forensic Laboratory
local.contributor.affiliationSuann, Craig J, Racing New South Wales
local.contributor.affiliationMcLeod, Malcolm, College of Physical and Mathematical Sciences, ANU
local.contributor.authoruidMcLeod, Malcolm, u4045340
local.description.embargo2037-12-31
local.description.notesImported from ARIES
local.identifier.absfor039902 - Forensic Chemistry
local.identifier.ariespublicationu4005981xPUB267
local.identifier.citationvolume813
local.identifier.doi10.1016/j.jchromb.2004.09.052
local.identifier.scopusID2-s2.0-8844256614
local.type.statusPublished Version

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