Influence of Nano-Sized SiC on the Laser Powder Bed Fusion of Molybdenum

Authors

Ellsworth, Nathan E.
Kemnitz, Ryan A.
Eckley, Cayla C.
Sexton, Brianna M.
Bowers, Cynthia T.
Machacek, Joshua
Burggraf, Larry W.

Journal Title

Journal ISSN

Volume Title

Publisher

MDPI

Abstract

Consolidation of pure molybdenum through laser powder bed fusion and other additive manufacturing techniques is complicated by a high melting temperature, thermal conductivity and ductile-to-brittle transition temperature. Nano-sized SiC particles (0.1 wt%) were homogeneously mixed with molybdenum powder and the printing characteristics, chemical composition, microstructure, mechanical properties were compared to pure molybdenum for scan speeds of 100, 200, 400, and 800 mm/s. The addition of SiC improved the optically determined density and flexural strength at 400 mm/s by 92% and 80%, respectively. The oxygen content was reduced by an average of 52% over the four scan speeds analyzed. Two mechanisms of oxygen reduction were identified as responsible for the improvements: oxidation of free carbon and the creation of secondary phase nanoparticles. This study illustrates the promising influence of nanoparticle additions to refractory metals in laser powder bed fusion.

Description

Keywords

Citation

Source

Crystals

Book Title

Entity type

Access Statement

Open Access

License Rights

Creative Commons Attribution (CC BY)

Restricted until

Downloads