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A Rapid and Straightforward Supramolecular Self-Assembly Experiment to Prepare and Characterize a Triple Helicate Complex

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Date

2018

Authors

White, Nicholas

Journal Title

Journal ISSN

Volume Title

Publisher

American Chemical Society

Abstract

This experiment prepares a large (Mr: 1821 g mol–1) triple helicate complex quickly in one pot from inexpensive starting materials. The protocol illustrates the power of self-assembly in a simple manner that is suitable for second-year general chemistry students using reversible imine bond and metal–ligand bond formation. Plastic molecular models and 1H NMR spectroscopy are used to elucidate the structure of the self-assembled product.

Description

Keywords

Citation

URI

http://hdl.handle.net/1885/164039

Collections

ANU Research Publications

Source

Journal of Chemical Education

Type

Journal article

Book Title

Entity type

Access Statement

License Rights

DOI

10.1021/acs.jchemed.7b00674

Restricted until

2037-12-31

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Description
01_White_A_Rapid_and_Straightforward_2018.pdf (3.27 MB)

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