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Rapid pulse length determination in high-resolution NMR

Date

Authors

Wu, Peter

Otting, Gottfried

Publisher

Academic Press

Abstract

A nutation method that delivers the 90°(1H) pulse length in a single scan was investigated. The method was found to produce accurate results with an accuracy of about 0.5% under the stringent conditions of high-resolution NMR spectroscopy for different s

Keywords

Keywords: Automation; Couplings; Data acquisition; Deuterium compounds; Fourier transforms; Magnetic resonance imaging; Spectrometers; 90° pulse; Homo-gated decoupling; Nutation spectroscopy; Radiofrequency (RF) irradiation; Nuclear magnetic resonance; lysozyme; an 90°pulse; Automation; Homo-gated decoupling; Nutation spectroscopy

URI

http://hdl.handle.net/1885/82010

Collections

ANU Research Publications

Source

Journal of Magnetic Resonance

Type

Journal article

DOI

10.1016/j.jmr.2005.05.018

Restricted until

2037-12-31

Downloads

File

Description

01_Wu_Rapid_pulse_length_2005.pdf (274.76 KB)