Resolution of (±)-nipecotic acid ((±)-3-piperidinecarboxylic acid) by separation of palladium(II) diastereomers containing orthometallated (S)-(-)-1-[1-(dimethylamino)ethyl]naphthalene

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dc.contributor.authorGugger, Paul
dc.contributor.authorHockless, David
dc.contributor.authorKilah, Nathan
dc.contributor.authorMayadunne, Roshan
dc.contributor.authorWild, Stanley (Bruce)
dc.date.accessioned2015-12-10T22:27:03Z
dc.date.issued2008
dc.date.updated2015-12-09T09:37:17Z
dc.description.abstractAn efficient resolution of (±)-nipecotic acid has been achieved by the fractional crystallization of internally diastereomeric palladium(II) complexes containing the chelated carboxylate and orthometallated (S)-(-)-1-[1-(dimethylamino)ethyl]naphthalene.
dc.identifier.issn0957-4166
dc.identifier.urihttp://hdl.handle.net/1885/54028
dc.publisherPergamon-Elsevier Ltd
dc.sourceTetrahedron: Asymmetry
dc.subjectKeywords: 1 [1 (dimethylamino)ethyl]naphthalene; hydrochloric acid; naphthalene derivative; nipecotic acid; nipecotic acid (3 piperidinecarboxylic acid); palladium; article; chemical structure; crystallization; enantiomer; priority journal; proton nuclear magnetic
dc.titleResolution of (±)-nipecotic acid ((±)-3-piperidinecarboxylic acid) by separation of palladium(II) diastereomers containing orthometallated (S)-(-)-1-[1-(dimethylamino)ethyl]naphthalene
dc.typeJournal article
local.bibliographicCitation.issue15
local.bibliographicCitation.lastpage1812
local.bibliographicCitation.startpage1810
local.contributor.affiliationGugger, Paul, College of Physical and Mathematical Sciences, ANU
local.contributor.affiliationHockless, David, College of Physical and Mathematical Sciences, ANU
local.contributor.affiliationKilah, Nathan, College of Physical and Mathematical Sciences, ANU
local.contributor.affiliationMayadunne, Roshan, College of Physical and Mathematical Sciences, ANU
local.contributor.affiliationWild, Stanley (Bruce), College of Physical and Mathematical Sciences, ANU
local.contributor.authoruidGugger, Paul, u8000186
local.contributor.authoruidHockless, David, u930167
local.contributor.authoruidKilah, Nathan, u4101782
local.contributor.authoruidMayadunne, Roshan, u920523
local.contributor.authoruidWild, Stanley (Bruce), u7901996
local.description.embargo2037-12-31
local.description.notesImported from ARIES
local.identifier.absfor030204 - Main Group Metal Chemistry
local.identifier.ariespublicationu4217927xPUB289
local.identifier.citationvolume19
local.identifier.doi10.1016/j.tetasy.2008.07.018
local.identifier.scopusID2-s2.0-49049088285
local.identifier.thomsonID000259623600008
local.type.statusPublished Version

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