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Structures and Phase Transitions in (MoO 2 ) 2 P 2 O 7

Lister, Sarah E; Soleilhavoup, Anne; Withers, Raymond; Hodgkinson, Paul; Evans, John S O

Description

We report structural investigations into (MoO2) 2P2O7 using a combination of X-ray, neutron and electron diffraction, and solid-state NMR supported by first principles quantum chemical calculations. These reveal a series of phase transitions on cooling at temperatures of 377 and 325 K. The high temperature y-phase has connectivity consistent with that proposed by Kierkegaard at room temperature (but with improved bond length distribution), and contains 13 unique atoms in space group Prima with...[Show more]

CollectionsANU Research Publications
Date published: 2010
Type: Journal article
URI: http://hdl.handle.net/1885/58682
Source: Inorganic Chemistry
DOI: 10.1021/ic902166j

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