Multi-component assembly of the bicyclic core associated with the tRNA synthetase inhibitors SB-203207 and SB-203208. Application to the synthesis of biologically active analogues
Banwell, Martin; Crasto, Curtis; Easton, Christopher; Karoli, Tomislav; March, Darren; Nairn, Michael; O'Hanlon, Peter; Oldham, Mark; Willis, Anthony; Yue, Weimin
The ketone (±)-5, which embodies the bicyclic core associated with the title tRNA synthetase inhibitors 1 and 2, has been prepared via a three-component coupling reaction involving 2-(hydroxymethyl)cyclopent-2-enone (15), methylamine (6) and propiolamide
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