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Structural Changes of MoS 2 Nano-powder in Dependence on the Annealing Temperature

Berdinsky, A.S.; Chadderton, Lewis; Yoo, J B; Gutakovsky, A.K.; Fedorov, V.E.; Mazalov, L N; Fink, Dietmar

Description

To search for structural changes of molybdenum disulphide (MoS2) nano-powder under thermal treatment, the annealing of the powder was carried out in vacuum or in argon. MoS2 powder with a grain size of 3-5 nm was synthesized by a chemical method. The temperature of annealing was varied in the range of 380-1000 °C. The time of annealing was varied in the range from 4 h (380 °C) to 5 min (1000 °C). X-ray diffraction and transmission electron microscopy analyses were made to see the character of...[Show more]

CollectionsANU Research Publications
Date published: 2005
Type: Journal article
URI: http://hdl.handle.net/1885/82307
Source: Applied Physics A: Materials Science and Processing
DOI: 10.1007/S00339-004-3003-5

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