Guaiacol transprotection: replacement of the phenoxy isopropyl protecting function by acetyl
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Williams, Craig; Mander, Lewis
Description
A one-step method for the conversion of isopropyl protected guaiacols to the corresponding acetates is reported. Treating 6-substituted isopropyl protected guaiacols with trimethylsilyl trifluoromethanesulfonate in a mixture of acetic anhydride and acetonitrile affords 6-substituted guaiacol acetates in yields ranging from 35% to 99%.
Collections | ANU Research Publications |
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Date published: | 2004 |
Type: | Journal article |
URI: | http://hdl.handle.net/1885/78384 |
Source: | Tetrahedron Letters |
DOI: | 10.1016/j.tetlet.2003.11.065 |
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