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Guaiacol transprotection: replacement of the phenoxy isopropyl protecting function by acetyl

Williams, Craig; Mander, Lewis

Description

A one-step method for the conversion of isopropyl protected guaiacols to the corresponding acetates is reported. Treating 6-substituted isopropyl protected guaiacols with trimethylsilyl trifluoromethanesulfonate in a mixture of acetic anhydride and acetonitrile affords 6-substituted guaiacol acetates in yields ranging from 35% to 99%.

CollectionsANU Research Publications
Date published: 2004
Type: Journal article
URI: http://hdl.handle.net/1885/78384
Source: Tetrahedron Letters
DOI: 10.1016/j.tetlet.2003.11.065

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