In situ electrochemical-NMR spectroscopy. Reduction of aromatic halides
A three-electrode, two-compartment cylindrical electrochemical cell has been constructed for in situ operation in a 500 MHz 1H NMR spectrometer. The cell was designed around a standard 10-mm sample tube holder and is lowered into position within the magnet by height-adjustable aluminum rods that support the wires connecting the potentiostat to the working, auxiliary and reference electrodes. The electrochemical cell functions under diffusion-controlled conditions in nonspinning mode and is able...[Show more]
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