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5-Nitrosalicylic acid and its proton-transfer compounds with aliphatic Lewis bases

Smith, Graham; Hartono, Andy; Wen, Daying; Healy, Peter; White, Jonathan; Rae, A David


The crystal structures of the proton-transfer compounds of 5-nitrosalicylic acid (5-nsa) with morpholine (morph), hexamethylenetetraminc (hmt), and ethylenediamine (en) have been determined and their solid-state packing structures described. The compounds are [(morph)+(5-nsa) -] 1, [(hmt)+(5-nsa)-·H2O] 2, and [(en)2+(5-nsa)-·H2O] 3. In all compounds, protonation of the hetero-nitrogen of the Lewis base occurs. With 1, the 5-nsa anions and the morpholine cations lie, respectively, in or across...[Show more]

CollectionsANU Research Publications
Date published: 2005
Type: Journal article
Source: Australian Journal of Chemistry
DOI: 10.1071/CH04144


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