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Simple method for the handling of crystals at low temperature: Application to the X-ray structure determination of Bu t 2 P(=NSiMe 3 )NHSiMe 3 and Bu t 2 P(NSiMe 3 ) 2

Edwards, Alison; Wenger, Eric

Description

Crystals of the very soluble iminophosphonamide species Bu2tP(=NSiMe3)NHSiMe3 (1) and [But2P(NSiMe3)2]Li·(thf)2 (2) have been obtained and were mounted at dry-ice temperature using a propan-2-ol matrix for X-ray data collection at 100 K. This very simple

CollectionsANU Research Publications
Date published: 2002
Type: Journal article
URI: http://hdl.handle.net/1885/72492
Source: Australian Journal of Chemistry
DOI: 10.1071/CH02016

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