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Application of a Raney-cobalt-mediated tandem reductive cyclization protocol to total syntheses of the aspidosperma alkaloids (±)- limaspermidine and (±)-1-acetylaspidoalbidine

Tan, Shen Hui-Xian; Banwell, Martin; Willis, Anthony; Reekie, Tristan


The racemic modification of the Aspidosperma alkaloid limaspermidine (1) has been prepared in ten steps including one involving a Raney-cobalt-mediated tandem reductive cyclization of nitrile 8 to give the tetracyclic system 9b. Compound (±)-1 has been c

CollectionsANU Research Publications
Date published: 2012
Type: Journal article
Source: Organic Letters
DOI: 10.1021/ol3026846


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