Yeo, Joey; Cheah, Michael; Bondin, Mark I.; Best, Stephen Peter
The design and operation of electrosynthesis cells for generation of samples for X-ray absorption spectroscopy are described. Optimization of continuous-flow methods allows the generation of highly reducing species, which may be combined with spectroscopic validation of the composition of the electrogenerated solution. It is shown that the large sample volume (10mL) of the 110mM (in the absorbing element) solution required for such experiments can be reduced to ∼100L using a strategy in which...[Show more]
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