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Superstructure of mullite-type KAl 9 O 14

Lazic, Biljana; Kruger, Hannes; Kaindl, Reinhard; Perfler, Lukas; Kremenović, Aleksandar; Cvetković, Vladica; Withers, Raymond

Description

Large whiskers of a new KAl9O14 polymorph with mullite-type structure were synthesized. The chemical composition of the crystals was confirmed by energy-dispersive X-ray spectroscopy, and the structure was determined using single-crystal X-ray diffraction. Nanosized twin domains and one-dimensional diffuse scattering were observed utilizing transmission electron microscopy. The compound crystallizes in space group P21/n (a = 8.1880(8), b = 7.6760(7), c = 8.7944(9) Å, β = 110.570(8), V =...[Show more]

CollectionsANU Research Publications
Date published: 2013
Type: Journal article
URI: http://hdl.handle.net/1885/63052
Source: Chemistry of Materials
DOI: 10.1021/cm3038476

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