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Resolution of (±)-nipecotic acid ((±)-3-piperidinecarboxylic acid) by separation of palladium(II) diastereomers containing orthometallated (S)-(-)-1-[1-(dimethylamino)ethyl]naphthalene

Gugger, Paul; Hockless, David; Kilah, Nathan; Mayadunne, Roshan; Wild, Stanley (Bruce)

Description

An efficient resolution of (±)-nipecotic acid has been achieved by the fractional crystallization of internally diastereomeric palladium(II) complexes containing the chelated carboxylate and orthometallated (S)-(-)-1-[1-(dimethylamino)ethyl]naphthalene.

CollectionsANU Research Publications
Date published: 2008
Type: Journal article
URI: http://hdl.handle.net/1885/54028
Source: Tetrahedron: Asymmetry
DOI: 10.1016/j.tetasy.2008.07.018

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