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Molybdenum and rhenium disulfide synthesis via high-pressure carbonate melt

Anenburg, Michael

Description

Various applications of transition metal dichalcogenides (TMDs) require preparation by exfoliation of precursor bulk materials. However, bulk TMDs are not always available in suitable forms and current synthesis methods may not result in appropriate crystals. This study reports synthesis of large crystals (50–100 μm) of MoS2 and ReS2, by recrystallisation of MoS2 powder or reaction of sulfate with perrhenic acid, respectively. The reactions have been performed at high pressure and temperature...[Show more]

CollectionsANU Research Publications
Date published: 2019-04-08
Type: Journal article
URI: http://hdl.handle.net/1885/202349
Source: CrystEngComm
DOI: 10.1039/c9ce00188c

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