High-Yield Electrochemical Production of Large-Sized and Thinly Layered NiPS3 Flakes for Overall Water Splitting
Achieving large‐sized and thinly layered 2D metal phosphorus trichalcogenides with high quality and yield has been an urgent quest due to extraordinary physical/chemical characteristics for multiple applications. Nevertheless, current preparation methodologies suffer from uncontrolled thicknesses, uneven morphologies and area distributions, long processing times, and inferior quality. Here, a sonication‐free and fast (in minutes) electrochemical cathodic exfoliation approach is reported that...[Show more]
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